Assessment of absorber composition and nanocrystalline phases in CuInS2 based photovoltaic technologies by ex-situ/in-situ resonant Raman scattering measurements
Identifieur interne : 003409 ( Main/Repository ); précédent : 003408; suivant : 003410Assessment of absorber composition and nanocrystalline phases in CuInS2 based photovoltaic technologies by ex-situ/in-situ resonant Raman scattering measurements
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Abstract
This work describes the use of quasi-resonant Raman scattering measurements for the assessment of chemical composition and nanocrystalline phases in CuInS2 based photovoltaic technologies. Raman spectra measured in S-rich CuIn(S,Se)2 layers at a fixed wavelength of 785 nm show a strong increase in the intensity of the peaks that are related to the quasi-resonant excitation of the corresponding vibrational modes. The spectra measured at these conditions are characterised by the presence of seven bands that have been identified with four first order peaks in the 200-400 cm-1 spectral region and three second order peaks in the 550-750 cm-1 spectral region. These spectra are strongly sensitive to changes in the composition of S-rich Culn(Se,S)2 alloys. On the other hand, the strong increase in the intensity of the peaks allows the development of in-situ measurements for real time process monitoring. As an example of this application, Raman spectra have been measured at real time conditions during the growth of colloidal CuInS2 nanocrystals that are being developed for the fabrication of low cost solar cells. The data obtained corroborate the potential of quasi-resonant Raman scattering measurements for the development of ex-situ and in-situ quality control and process monitoring tools in thin film chalcopyrite photovoltaic technologies.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Assessment of absorber composition and nanocrystalline phases in CuInS<sub>2</sub> based photovoltaic technologies by ex-situ/in-situ resonant Raman scattering measurements</title><author><name sortKey="Izquierdo Roca, V" uniqKey="Izquierdo Roca V">V. Izquierdo-Roca</name><affiliation wicri:level="2"><inist:fA14 i1="01"><s1>IN2UB/Departament d'Electrònica, Universitat de Barcelona, C. Martí i Franquès 1</s1><s2>08028 Barcelona</s2><s3>ESP</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation></author><author><name sortKey="Shavel, A" uniqKey="Shavel A">A. Shavel</name><affiliation wicri:level="2"><inist:fA14 i1="01"><s1>IN2UB/Departament d'Electrònica, Universitat de Barcelona, C. Martí i Franquès 1</s1><s2>08028 Barcelona</s2><s3>ESP</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation></author><author><name sortKey="Saucedo, E" uniqKey="Saucedo E">E. Saucedo</name><affiliation wicri:level="2"><inist:fA14 i1="02"><s1>IREC, Catalonia Institute for Energy Research, C. Jardins de les Dones de Negre 1</s1><s2>08930 Sant Adrià del Besbs, Barcelona</s2><s3>ESP</s3><sZ>3 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation></author><author><name sortKey="Jaime Ferrer, S" uniqKey="Jaime Ferrer S">S. Jaime-Ferrer</name><affiliation wicri:level="3"><inist:fA14 i1="03"><s1>NEXCIS, Zone Industrielle 190 Av. Celestin Coq</s1><s2>13790 Rousset</s2><s3>FRA</s3><sZ>4 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Provence-Alpes-Côte d'Azur</region><settlement type="city">Rousset</settlement></placeName></affiliation></author><author><name sortKey="Alvarez Garcia, J" uniqKey="Alvarez Garcia J">J. Alvarez-Garcia</name><affiliation wicri:level="2"><inist:fA14 i1="04"><s1>Centre de Recerca i Investigació de Catalunya (CRIC), Trav. de Gràcia 108</s1><s2>08012 Barcelona</s2><s3>ESP</s3><sZ>5 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation></author><author><name sortKey="Cabot, A" uniqKey="Cabot A">A. Cabot</name><affiliation wicri:level="2"><inist:fA14 i1="01"><s1>IN2UB/Departament d'Electrònica, Universitat de Barcelona, C. Martí i Franquès 1</s1><s2>08028 Barcelona</s2><s3>ESP</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation><affiliation wicri:level="2"><inist:fA14 i1="02"><s1>IREC, Catalonia Institute for Energy Research, C. Jardins de les Dones de Negre 1</s1><s2>08930 Sant Adrià del Besbs, Barcelona</s2><s3>ESP</s3><sZ>3 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation></author><author><name sortKey="Perez Rodriguez, A" uniqKey="Perez Rodriguez A">A. Perez-Rodriguez</name><affiliation wicri:level="2"><inist:fA14 i1="01"><s1>IN2UB/Departament d'Electrònica, Universitat de Barcelona, C. Martí i Franquès 1</s1><s2>08028 Barcelona</s2><s3>ESP</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation><affiliation wicri:level="2"><inist:fA14 i1="02"><s1>IREC, Catalonia Institute for Energy Research, C. Jardins de les Dones de Negre 1</s1><s2>08930 Sant Adrià del Besbs, Barcelona</s2><s3>ESP</s3><sZ>3 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation></author><author><name sortKey="Bermudez, V" uniqKey="Bermudez V">V. Bermudez</name><affiliation wicri:level="3"><inist:fA14 i1="03"><s1>NEXCIS, Zone Industrielle 190 Av. Celestin Coq</s1><s2>13790 Rousset</s2><s3>FRA</s3><sZ>4 aut.</sZ><sZ>8 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Provence-Alpes-Côte d'Azur</region><settlement type="city">Rousset</settlement></placeName></affiliation></author><author><name sortKey="Morante, J R" uniqKey="Morante J">J. R. Morante</name><affiliation wicri:level="2"><inist:fA14 i1="01"><s1>IN2UB/Departament d'Electrònica, Universitat de Barcelona, C. Martí i Franquès 1</s1><s2>08028 Barcelona</s2><s3>ESP</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation><affiliation wicri:level="2"><inist:fA14 i1="02"><s1>IREC, Catalonia Institute for Energy Research, C. Jardins de les Dones de Negre 1</s1><s2>08930 Sant Adrià del Besbs, Barcelona</s2><s3>ESP</s3><sZ>3 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></inist:fA14><country>Espagne</country><placeName><region nuts="2" type="communauté">Catalogne</region></placeName></affiliation></author></titleStmt><publicationStmt><idno type="inist">11-0266022</idno><date when="2011">2011</date><idno type="stanalyst">PASCAL 11-0266022 INIST</idno><idno type="RBID">Pascal:11-0266022</idno><idno type="wicri:Area/Main/Corpus">003021</idno><idno type="wicri:Area/Main/Repository">003409</idno></publicationStmt><seriesStmt><idno type="ISSN">0927-0248</idno><title level="j" type="abbreviated">Sol. energy mater. sol. cells</title><title level="j" type="main">Solar energy materials and solar cells</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Absorbent material</term><term>Chalcopyrite</term><term>Chemical composition</term><term>Copper sulfide</term><term>Cost lowering</term><term>First order</term><term>In situ</term><term>Indium sulfide</term><term>Monitoring</term><term>Nanocrystal</term><term>Quality control</term><term>Raman scattering</term><term>Real time</term><term>Solar cell</term><term>Ternary compound</term><term>Thin film</term><term>Vibrational mode</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Matériau absorbant</term><term>In situ</term><term>Diffusion Raman</term><term>Composition chimique</term><term>Mode vibration</term><term>Ordre 1</term><term>Temps réel</term><term>Monitorage</term><term>Diminution coût</term><term>Cellule solaire</term><term>Contrôle qualité</term><term>Nanocristal</term><term>Composé ternaire</term><term>Sulfure de cuivre</term><term>Sulfure d'indium</term><term>Couche mince</term><term>Chalcopyrite</term><term>CuInS2</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">This work describes the use of quasi-resonant Raman scattering measurements for the assessment of chemical composition and nanocrystalline phases in CuInS<sub>2</sub> based photovoltaic technologies. Raman spectra measured in S-rich CuIn(S,Se)<sub>2</sub> layers at a fixed wavelength of 785 nm show a strong increase in the intensity of the peaks that are related to the quasi-resonant excitation of the corresponding vibrational modes. The spectra measured at these conditions are characterised by the presence of seven bands that have been identified with four first order peaks in the 200-400 cm<sup>-1</sup> spectral region and three second order peaks in the 550-750 cm<sup>-1</sup> spectral region. These spectra are strongly sensitive to changes in the composition of S-rich Culn(Se,S)<sub>2</sub> alloys. On the other hand, the strong increase in the intensity of the peaks allows the development of in-situ measurements for real time process monitoring. As an example of this application, Raman spectra have been measured at real time conditions during the growth of colloidal CuInS<sub>2</sub> nanocrystals that are being developed for the fabrication of low cost solar cells. The data obtained corroborate the potential of quasi-resonant Raman scattering measurements for the development of ex-situ and in-situ quality control and process monitoring tools in thin film chalcopyrite photovoltaic technologies.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0927-0248</s0></fA01><fA03 i2="1"><s0>Sol. energy mater. sol. cells</s0></fA03><fA05><s2>95</s2></fA05><fA06><s3>SUP1</s3></fA06><fA08 i1="01" i2="1" l="ENG"><s1>Assessment of absorber composition and nanocrystalline phases in CuInS<sub>2</sub> based photovoltaic technologies by ex-situ/in-situ resonant Raman scattering measurements</s1></fA08><fA09 i1="01" i2="1" l="ENG"><s1>Thin Film Photovoltaic Applications (TFPA)</s1></fA09><fA11 i1="01" i2="1"><s1>IZQUIERDO-ROCA (V.)</s1></fA11><fA11 i1="02" i2="1"><s1>SHAVEL (A.)</s1></fA11><fA11 i1="03" i2="1"><s1>SAUCEDO (E.)</s1></fA11><fA11 i1="04" i2="1"><s1>JAIME-FERRER (S.)</s1></fA11><fA11 i1="05" i2="1"><s1>ALVAREZ-GARCIA (J.)</s1></fA11><fA11 i1="06" i2="1"><s1>CABOT (A.)</s1></fA11><fA11 i1="07" i2="1"><s1>PEREZ-RODRIGUEZ (A.)</s1></fA11><fA11 i1="08" i2="1"><s1>BERMUDEZ (V.)</s1></fA11><fA11 i1="09" i2="1"><s1>MORANTE (J. R.)</s1></fA11><fA12 i1="01" i2="1"><s1>ESCOUBAS (Ludovic)</s1><s9>ed.</s9></fA12><fA12 i1="02" i2="1"><s1>CHOPRA (Kasturi)</s1><s9>ed.</s9></fA12><fA12 i1="03" i2="1"><s1>JEANNEROT (Luc)</s1><s9>ed.</s9></fA12><fA12 i1="04" i2="1"><s1>CHARRIER (Véronique)</s1><s9>ed.</s9></fA12><fA14 i1="01"><s1>IN2UB/Departament d'Electrònica, Universitat de Barcelona, C. Martí i Franquès 1</s1><s2>08028 Barcelona</s2><s3>ESP</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></fA14><fA14 i1="02"><s1>IREC, Catalonia Institute for Energy Research, C. Jardins de les Dones de Negre 1</s1><s2>08930 Sant Adrià del Besbs, Barcelona</s2><s3>ESP</s3><sZ>3 aut.</sZ><sZ>6 aut.</sZ><sZ>7 aut.</sZ><sZ>9 aut.</sZ></fA14><fA14 i1="03"><s1>NEXCIS, Zone Industrielle 190 Av. Celestin Coq</s1><s2>13790 Rousset</s2><s3>FRA</s3><sZ>4 aut.</sZ><sZ>8 aut.</sZ></fA14><fA14 i1="04"><s1>Centre de Recerca i Investigació de Catalunya (CRIC), Trav. de Gràcia 108</s1><s2>08012 Barcelona</s2><s3>ESP</s3><sZ>5 aut.</sZ></fA14><fA15 i1="01"><s1>Aix-Marseille University, Institut des Matériaux Microélectronique Nanosciences de Provence, IM2NP-UMR CNRS 6242</s1><s2>Marseille-Toulon</s2><s3>FRA</s3><sZ>1 aut.</sZ></fA15><fA18 i1="01" i2="1"><s1>POPsud</s1><s2>Marseille</s2><s3>FRA</s3><s9>org-cong.</s9></fA18><fA18 i1="02" i2="1"><s1>Université Paul Cézanne Aix Marseille III</s1><s3>FRA</s3><s9>org-cong.</s9></fA18><fA20><s2>S83-S88</s2></fA20><fA21><s1>2011</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>18016</s2><s5>354000191534860130</s5></fA43><fA44><s0>0000</s0><s1>© 2011 INIST-CNRS. All rights reserved.</s1></fA44><fA45><s0>24 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>11-0266022</s0></fA47><fA60><s1>P</s1><s2>C</s2></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>Solar energy materials and solar cells</s0></fA64><fA66 i1="01"><s0>NLD</s0></fA66><fC01 i1="01" l="ENG"><s0>This work describes the use of quasi-resonant Raman scattering measurements for the assessment of chemical composition and nanocrystalline phases in CuInS<sub>2</sub> based photovoltaic technologies. Raman spectra measured in S-rich CuIn(S,Se)<sub>2</sub> layers at a fixed wavelength of 785 nm show a strong increase in the intensity of the peaks that are related to the quasi-resonant excitation of the corresponding vibrational modes. The spectra measured at these conditions are characterised by the presence of seven bands that have been identified with four first order peaks in the 200-400 cm<sup>-1</sup> spectral region and three second order peaks in the 550-750 cm<sup>-1</sup> spectral region. These spectra are strongly sensitive to changes in the composition of S-rich Culn(Se,S)<sub>2</sub> alloys. On the other hand, the strong increase in the intensity of the peaks allows the development of in-situ measurements for real time process monitoring. As an example of this application, Raman spectra have been measured at real time conditions during the growth of colloidal CuInS<sub>2</sub> nanocrystals that are being developed for the fabrication of low cost solar cells. The data obtained corroborate the potential of quasi-resonant Raman scattering measurements for the development of ex-situ and in-situ quality control and process monitoring tools in thin film chalcopyrite photovoltaic technologies.</s0></fC01><fC02 i1="01" i2="X"><s0>001D06C02D1</s0></fC02><fC02 i1="02" i2="X"><s0>001D05I03D</s0></fC02><fC02 i1="03" i2="X"><s0>230</s0></fC02><fC03 i1="01" i2="X" l="FRE"><s0>Matériau absorbant</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="ENG"><s0>Absorbent material</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="SPA"><s0>Material absorbente</s0><s5>01</s5></fC03><fC03 i1="02" i2="X" l="FRE"><s0>In situ</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="ENG"><s0>In situ</s0><s5>02</s5></fC03><fC03 i1="02" i2="X" l="SPA"><s0>In situ</s0><s5>02</s5></fC03><fC03 i1="03" i2="X" l="FRE"><s0>Diffusion Raman</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="ENG"><s0>Raman scattering</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="SPA"><s0>Difusión Ramán</s0><s5>03</s5></fC03><fC03 i1="04" i2="X" l="FRE"><s0>Composition chimique</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="ENG"><s0>Chemical composition</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="SPA"><s0>Composición química</s0><s5>04</s5></fC03><fC03 i1="05" i2="X" l="FRE"><s0>Mode vibration</s0><s5>05</s5></fC03><fC03 i1="05" i2="X" l="ENG"><s0>Vibrational mode</s0><s5>05</s5></fC03><fC03 i1="05" i2="X" l="SPA"><s0>Modo de vibración</s0><s5>05</s5></fC03><fC03 i1="06" i2="X" l="FRE"><s0>Ordre 1</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="ENG"><s0>First order</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="SPA"><s0>Orden 1</s0><s5>06</s5></fC03><fC03 i1="07" i2="X" l="FRE"><s0>Temps réel</s0><s5>07</s5></fC03><fC03 i1="07" i2="X" l="ENG"><s0>Real time</s0><s5>07</s5></fC03><fC03 i1="07" i2="X" l="SPA"><s0>Tiempo real</s0><s5>07</s5></fC03><fC03 i1="08" i2="X" l="FRE"><s0>Monitorage</s0><s5>08</s5></fC03><fC03 i1="08" i2="X" l="ENG"><s0>Monitoring</s0><s5>08</s5></fC03><fC03 i1="08" i2="X" l="SPA"><s0>Monitoreo</s0><s5>08</s5></fC03><fC03 i1="09" i2="X" l="FRE"><s0>Diminution coût</s0><s5>09</s5></fC03><fC03 i1="09" i2="X" l="ENG"><s0>Cost lowering</s0><s5>09</s5></fC03><fC03 i1="09" i2="X" l="SPA"><s0>Reducción costes</s0><s5>09</s5></fC03><fC03 i1="10" i2="X" l="FRE"><s0>Cellule solaire</s0><s5>10</s5></fC03><fC03 i1="10" i2="X" l="ENG"><s0>Solar cell</s0><s5>10</s5></fC03><fC03 i1="10" i2="X" l="SPA"><s0>Célula solar</s0><s5>10</s5></fC03><fC03 i1="11" i2="X" l="FRE"><s0>Contrôle qualité</s0><s5>11</s5></fC03><fC03 i1="11" i2="X" l="ENG"><s0>Quality control</s0><s5>11</s5></fC03><fC03 i1="11" i2="X" l="SPA"><s0>Control de calidad</s0><s5>11</s5></fC03><fC03 i1="12" i2="X" l="FRE"><s0>Nanocristal</s0><s5>22</s5></fC03><fC03 i1="12" i2="X" l="ENG"><s0>Nanocrystal</s0><s5>22</s5></fC03><fC03 i1="12" i2="X" l="SPA"><s0>Nanocristal</s0><s5>22</s5></fC03><fC03 i1="13" i2="X" l="FRE"><s0>Composé ternaire</s0><s5>23</s5></fC03><fC03 i1="13" i2="X" l="ENG"><s0>Ternary compound</s0><s5>23</s5></fC03><fC03 i1="13" i2="X" l="SPA"><s0>Compuesto ternario</s0><s5>23</s5></fC03><fC03 i1="14" i2="X" l="FRE"><s0>Sulfure de cuivre</s0><s5>24</s5></fC03><fC03 i1="14" i2="X" l="ENG"><s0>Copper sulfide</s0><s5>24</s5></fC03><fC03 i1="14" i2="X" l="SPA"><s0>Cobre sulfuro</s0><s5>24</s5></fC03><fC03 i1="15" i2="X" l="FRE"><s0>Sulfure d'indium</s0><s5>25</s5></fC03><fC03 i1="15" i2="X" l="ENG"><s0>Indium sulfide</s0><s5>25</s5></fC03><fC03 i1="15" i2="X" l="SPA"><s0>Indio sulfuro</s0><s5>25</s5></fC03><fC03 i1="16" i2="X" l="FRE"><s0>Couche mince</s0><s5>26</s5></fC03><fC03 i1="16" i2="X" l="ENG"><s0>Thin film</s0><s5>26</s5></fC03><fC03 i1="16" i2="X" l="SPA"><s0>Capa fina</s0><s5>26</s5></fC03><fC03 i1="17" i2="X" l="FRE"><s0>Chalcopyrite</s0><s5>27</s5></fC03><fC03 i1="17" i2="X" l="ENG"><s0>Chalcopyrite</s0><s5>27</s5></fC03><fC03 i1="17" i2="X" l="SPA"><s0>Calcopirita</s0><s5>27</s5></fC03><fC03 i1="18" i2="X" l="FRE"><s0>CuInS2</s0><s4>INC</s4><s5>82</s5></fC03><fN21><s1>178</s1></fN21><fN44 i1="01"><s1>OTO</s1></fN44><fN82><s1>OTO</s1></fN82></pA><pR><fA30 i1="01" i2="1" l="ENG"><s1>Photovoltaic Technical Conference Thin Film 2010 (PVTC 2010)</s1><s2>1</s2><s3>Aix-en-Provence FRA</s3><s4>2010-05-27</s4></fA30></pR></standard></inist></record>Pour manipuler ce document sous Unix (Dilib)
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